| Title: | Pursuing the stabilisation of crystalline nanostructured magnetic manganites through a green low temperature hydrothermal synthesis |
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| Authors: | ID Minelli, Arianna, Dipartimento di Scienze Chimiche, Universita` degli Studi di Padova, via Marzolo 1, I-35131, Padova, Italy (Author)
ID Dolcet, Paolo, Dipartimento di Scienze Chimiche, Universita` degli Studi di Padova, via Marzolo 1, I-35131, Padova, Italy (Author)
ID Diodati, Stefano, Dipartimento di Scienze Chimiche, Universita` degli Studi di Padova, via Marzolo 1, I-35131, Padova, Italy (Author)
ID Gardonio, Sandra, Materials Research Laboratory, University of Nova Gorica, Vipavska 13, 5000 Nova Gorica, Slovenia (Author)
ID Innocenti, Claudia, Dipartimento di Chimica & RU Consorzio INSTM, Universita` di Firenze, via della Lastruccia 3-13, 50019, Sesto F.no (FI), Italy (Author)
ID Badocco, Denis, Dipartimento di Scienze Chimiche, Universita` degli Studi di Padova, via Marzolo 1, I-35131, Padova, Italy (Author)
ID Gialanella, Stefano, Dipartimento di Ingegneria Industriale, Universita` degli Studi di Trento, via Sommarive 9, I-38123, Trento, Italy (Author)
ID Pastore, Paolo, Dipartimento di Scienze Chimiche, Universita` degli Studi di Padova, via Marzolo 1, I-35131, Padova, Italy (Author)
ID Pandolfo, Luciano, Dipartimento di Scienze Chimiche, Universita` degli Studi di Padova, via Marzolo 1, I-35131, Padova, Italy (Author)
ID Caneschi, Andrea, Dipartimento di Chimica & RU Consorzio INSTM, Universita` di Firenze, via della Lastruccia 3-13, 50019, Sesto F.no (FI), Italy (Author)
ID Trapanati, Angela, CNR-Istituto Officina dei Materiali-Perugia, Via A. Pascoli, I-06123 Perugia, Italy (Author)
ID Gross, Silvia, Dipartimento di Scienze Chimiche, Universita` degli Studi di Padova, via Marzolo 1, I-35131, Padova, Italy (Author) |
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| Files: |
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| Language: | English |
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| Work type: | Not categorized |
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| Typology: | 1.01 - Original Scientific Article |
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| Organization: | UNG - University of Nova Gorica
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| Abstract: | A quick, easy and green water-based synthesis protocol involving coprecipitation of oxalates combined with hydrothermal treatment resulted in the crystallisation of nanostructured manganites at a relatively low temperature (180 °C). The subcritical hydrothermal approach was shown to play a key role in stabilising phases which are generally achieved at much higher temperatures and under harsher conditions, thus disclosing an exciting alternative for their synthesis. Through this mild wet chemistry approach, the compounds CuMnO2, ZnMn2O4 and ZnMnO3 were synthesised as nanocrystalline powders. Noticeably, the optimised route proved to be effective in stabilising the exotic polymorph cubic spinel ZnMnO3 in pure form. This is particularly notable, as very few records concerning this compound are available in the literature. The compounds were fully characterised from compositional, structural, morphological and magnetic points of view. |
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| Keywords: | nanostructured manganites, low temperature wet chemistry synthesis |
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| Year of publishing: | 2017 |
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| Number of pages: | 5 |
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| Numbering: | 10, 2 |
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| PID: | 20.500.12556/RUNG-3040-5f03e4f0-7145-7c7c-aa34-ee641257f99f |
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| COBISS.SI-ID: | 4759803 |
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| NUK URN: | URN:SI:UNG:REP:6HRJHEMD |
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| Publication date in RUNG: | 28.03.2017 |
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| Views: | 4292 |
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| Downloads: | 0 |
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