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Optimization of PTD system for characterization of transparent and semi-transparent samples
Hanna Budasheva, Dorota Korte, Mladen Franko, 2022, published scientific conference contribution abstract

Keywords: beam deflection spectrometry, materials characterisation, procedure optimisation
Published in RUNG: 01.07.2022; Views: 2498; Downloads: 8
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Natural precursor based hydrothermal synthesis of sodium carbide for reactor applications
Mohanachandran Nair Sindhu Swapna, 2017, original scientific article

Abstract: Carbides are a class of materials with high mechanical strength and refractory nature which finds a wide range of applications in industries and nuclear reactors. The existing synthesis methods of all types of carbides have problems in terms of use of toxic chemical precursors, high-cost, etc. Sodium carbide (Na2C2) which is an alkali metal carbide is the least explored one and also that there is no report of low-cost and low-temperature synthesis of sodium carbide using the eco-friendly, easily available natural precursors. In the present work, we report a simple low-cost, non-toxic hydrothermal synthesis of refractory sodium carbide using the natural precursor—Pandanus. The formation of sodium carbide along with boron carbide is evidenced by the structural and morphological characterizations. The sample thus synthesized is subjected to field emission scanning electron microscopy (FESEM), x-ray powder diffraction (XRD), ultraviolet (UV)—visible spectroscopy, Fourier transform infrared spectroscopy (FTIR), Raman, and photoluminescent (PL) spectroscopic techniques.
Keywords: sodium carbide, pandanus, hydrothermal synthesis, porous materials
Published in RUNG: 30.06.2022; Views: 3354; Downloads: 0
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Monitoring of chemical processes at the atomic level by X-ray absorption spectrometry using extremely bright synchrotron radiation sources
Iztok Arčon, invited lecture at foreign university

Abstract: X-ray absorption spectroscopy (XAS) is a powerful tool for characterisation of local structure and chemical state of selected elements in different new functional materials and biological or environmental samples. The XAS spectroscopy is based on extremely bright synchrotron radiation X-rays sources, which allow precise characterisation of bulk, nanostructured or highly diluted samples. The rapid development of extremely bright synchrotron sources of X-ray and ultraviolet light in recent years has opened new possibilities for research of matter at the atomic or molecular level, indispensable in the development of new functional nanostructured materials with desired properties. The lecture will present the possibilities offered by X-ray absorption spectroscopy with synchrotron light for ex-situ and in-situ or operando characterization of various functional porous and other nanomaterials before, after and during their operation.
Keywords: XAS, operando XANES, EXAFS, functional materials
Published in RUNG: 01.06.2022; Views: 2626; Downloads: 0
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Magnetic materials : GIAN Course 2022. Course name: Functional Materials
Blaž Belec, invited lecture at foreign university

Keywords: magnetic materials, nanomaterials, permanent magnets
Published in RUNG: 28.02.2022; Views: 2704; Downloads: 0
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Characterization of materials : GIAN Course 2022. Course name: Functional Materials
Blaž Belec, invited lecture at foreign university

Keywords: materials characterization
Published in RUNG: 28.02.2022; Views: 2462; Downloads: 0
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