1. System and method for continuous wave low power laser based synthesis of metal nano particles : patent certificate IN 512589, 2024-02-20Sankaranarayana Iyer Sankararaman, Mohanachandran Nair Sindhu Swapna, Abdul Rahim Sajeela Beevi Ashik, Ramachandran Nair Amba Devi Krishnanunni, Vadakkedathu Parameswaran Narayanan Nampoori, 2024, patent Opis: This disclosure relates to synthesis of metal nanoparticles (NPs). In particular, the invention relates to methods of synthesizing metal nanoparticles using Laser. The invention relates to Laser assisted synthesis of metal nanoparticles using continuous wave low laser power in a liquid medium. The system [100] for synthesis of metal nanoparticles, comprises of a laser source [101], a mechanical chopper [102], a lens [103], a target metal [104], a liquid medium [106] and a heat source [107]. Additionally the invention relates to laser assisted synthesis of metal nanoparticles with silver as the metal target and water as the liquid medium. The NPs produced are characterized by UV-Visible spectrophotometer, Field-emission Scanning Electron Microscope (FESEM), Energy Dispersive X-Ray Spectroscopy (EDS), and Transmission Electron Microscopy (TEM).Figure 1.
Ključne besede: cw laser, nanoparticle, method
Objavljeno v RUNG: 26.02.2024; Ogledov: 2421; Prenosov: 6
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2. Photoacoustics - A nondestructive evaluation technique for thermal and optical characterisation of metal mirrorsMohanachandran Nair Sindhu Swapna, NAMPOORI V P N, Sankararaman S, 2018, izvirni znanstveni članek Opis: Photoacoustic technique has emerged as a powerful tool for nondestructive evaluation and characterization. The high signal to noise ratio, sensitivity, and the least quantity of sample required make the technique suitable for wide range of applications. The intensity modulated laser beam focused on to the sample in the photoacoustic cell generates acoustic waves. Analysis of the acoustic signal enables the measurement of thermal and optical properties of the material. In the present work, the photoacoustic technique has been extended to find the thermal diffusivity and to demonstrate how the technique can be used for measuring optical reflection coefficient of a precious metal mirror—Aranmula mirror. The mirror being metal with high reflection coefficient, it finds application in optical instrumentation. The mirror is subjected to morphological characterization by atomic force microscopy and field emission scanning electron microscopy. The elemental and structural characterizations are done by energy dispersive x-ray spectroscopy, X-ray dot mapping, and X-Ray diffraction analysis. The fractal dimension of the particle distribution over the surface provides information about the surface roughness. The box-counting and power spectral fractal dimensions are found to be around 1.63 and 1.65 respectively.
Ključne besede: Photoacoustics, Nondestructive evaluation, Aranmula metal mirror, Reflectivity
Objavljeno v RUNG: 30.06.2022; Ogledov: 3331; Prenosov: 0
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