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System and method for continuous wave low power laser based synthesis of metal nano particles : patent certificate IN 512589, 2024-02-20
Sankaranarayana Iyer Sankararaman, Mohanachandran Nair Sindhu Swapna, Abdul Rahim Sajeela Beevi Ashik, Ramachandran Nair Amba Devi Krishnanunni, Vadakkedathu Parameswaran Narayanan Nampoori, 2024, patent

Opis: This disclosure relates to synthesis of metal nanoparticles (NPs). In particular, the invention relates to methods of synthesizing metal nanoparticles using Laser. The invention relates to Laser assisted synthesis of metal nanoparticles using continuous wave low laser power in a liquid medium. The system [100] for synthesis of metal nanoparticles, comprises of a laser source [101], a mechanical chopper [102], a lens [103], a target metal [104], a liquid medium [106] and a heat source [107]. Additionally the invention relates to laser assisted synthesis of metal nanoparticles with silver as the metal target and water as the liquid medium. The NPs produced are characterized by UV-Visible spectrophotometer, Field-emission Scanning Electron Microscope (FESEM), Energy Dispersive X-Ray Spectroscopy (EDS), and Transmission Electron Microscopy (TEM).Figure 1.
Ključne besede: cw laser, nanoparticle, method
Objavljeno v RUNG: 26.02.2024; Ogledov: 1671; Prenosov: 5
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2.
Ultralow duty cycle chopper instigated low power continuous wave laser assisted synthesis of silver nanoparticles : a novel approach
Mohanachandran Nair Sindhu Swapna, Abdul Rahim Sajeela Beevi Ashik, Ramachandran Nair Amba Devi Krishnanunni, Vadakkedathu Parameswaran Narayanan Nampoori, Sankaranarayana Iyer Sankararaman, 2020, izvirni znanstveni članek

Opis: This paper is the first report of advancement in the drastic reduction of the laser power density from 105 to 7.5 W/cm2 for the synthesis of silver nanoparticles (SNPs) using a low power (60 mW) continuous-wave (cw) laser and a specially designed ultralow duty cycle (3%) optical chopper wheel for modulating the laser beam at low frequencies (2 Hz). The target is irradiated by keeping it in a liquid medium at 40–60 °C to produce quantum dots to SNPs of size less than 40 nm. The UV-visible spectroscopic and electron microscopic analyses confirm the formation of quantum dots and SNPs of size-dependent bandgap energy varying from 1.92 to 2.37 eV. The photoluminescence studies not only support the above observations but also reveal the blue emission upon UV excitation through the chromaticity diagram. The proposed greener approach using the low power cw laser is cost-effective when compared with the high-power laser-assisted synthesis of SNPs reported until now.
Ključne besede: cw laser, silver nanoparticle, ultralow duty cycle, chopper
Objavljeno v RUNG: 30.06.2022; Ogledov: 2058; Prenosov: 27
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