Repozitorij Univerze v Novi Gorici

Iskanje po repozitoriju
A+ | A- | Pomoč | SLO | ENG

Iskalni niz: išči po
išči po
išči po
išči po
* po starem in bolonjskem študiju

Opcije:
  Ponastavi


11 - 18 / 18
Na začetekNa prejšnjo stran12Na naslednjo stranNa konec
11.
Identification of sweet cherry anthocyanins and hydroxycinnamic acids using HPLC coupled with DAD and MS detector
Polonca Trebše, Branka Mozetič Vodopivec, 2004, izvirni znanstveni članek

Opis: In absence of standards, HPLC coupled with DAD offers identification of polyphenols by scanning UV-Vis spectra of individual components, which spectral characteristics are unique, but not selective. At the same time HPLC-DAD determination methods of polyphenols differ in mobile phase solutions resulting in DAD scanned spectra deviation between different studies, aggravating the precise identification based on agreement to UV-Vis data from literature. Mass spectrometry (MS) detection with molar weight determination of the individual components in the sample enables more precise identification of compounds eluted from the column. Sweet cherry Petrovka polyphenols were separated on C18 Hypersil PEP 300 column (250 x 4.6 mm, 5 [mu]m) using gradient solvent mixture consisting of methanol, water and formic acid. MS and UV-Vis spectra of eluted anthocyanins and hydroxycinnamic acid were recorded. HPLC-MS analyses were performed using a LCQ [sup]TM ion trap, Finnigan, MAT mass spectrometer by atmospheric pressure chemical ionisation (ACPI). Molecular and fragmented ion masses of sweet cherry hydroxycinnamic acids and anthocyanins were determined and with UV-Vis spectra, in the range of 190-600 nm, used for identification of compounds. Electro spray mass spectrum of two hydroxycinnamic acids produced ions with m/z ratios of 353.0 and 337.0, which corresponded to molecular weights of neochlorogenic acid and 3'-p-coumarylquinic acid. The molecular weights of 5 anthocyanins corresponded to cyanidin-3-glucoside (449.0), cyanidin-3-rutinoside (595.1), peonidin-3-glucoside (463.1), pelargonidin-3-rutinoside (579.1) and peonidin-3-rlltinoside (609.2).
Ključne besede: češnje, antociani, hidroksicimetne kisline, HPLC-DAD/MS
Objavljeno v RUNG: 10.07.2015; Ogledov: 6724; Prenosov: 24
URL Povezava na celotno besedilo

12.
13.
14.
[Predstavitev znanstvenega dosežka Trans2Care] : v oddaji Tuttoggi, TV Koper Capodistria, 4. okt. 2013
2013, radijski ali tv dogodek

Ključne besede: prosti biblirubin, HPLC, TLS
Objavljeno v RUNG: 25.04.2014; Ogledov: 6403; Prenosov: 30
URL Povezava na celotno besedilo

15.
16.
17.
18.
Iskanje izvedeno v 0.03 sek.
Na vrh