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62.
NOVEL APPROACHES FOR THE DETERMINATION OF BIOGENIC AMINES IN FOOD SAMPLES
Mladen Franko, Mojca Žorž, Mitja Martelanc, Sara Budal, 2017, izvirni znanstveni članek

Opis: In this work, new analytical approaches for determination of biogenic amines in wines were developed. For the first time, we studied the derivatization of BAs in wines with naphthalene- 2,3-dicarboxaldehyde (NDA) and with dabsyl chloride (DBS) and analysis of derivatized BAs by HPLC coupled to fluorescence (HPLC-NDA-FL) and thermal lens spectrometry (HPLC-DBS-TLS) detectors. The sensitivity of the two methods (LODs HPLC-NDA-FL in the range 27-73 μg/L; LODs HPLC-DBS-TLS in the range 3.4-11 μg/L) was higher than that of the official method for biogenic amines in wines, OIV-MA-AS315-18 (60-77 μg/L). For its best performances, the HPLC-DBS-TLS technique was applied to the analysis of putrescine, cadaverine, histamine and tyramine in two white wine samples. Additionally, exploiting the Berthelot reaction, the TLS fast screening of biogenic amines in wines, following the release of ammonia by transglutaminase, was also proposed. This approach allowed us to determine total biogenic amount content in concentrations below 0.1 mg/L, expressed as equivalents of histamine.
Ključne besede: biogenic amines, NDA, liquid chromatography, TLS, fluorescence, wine
Objavljeno v RUNG: 02.11.2017; Ogledov: 5623; Prenosov: 278
.pdf Celotno besedilo (441,06 KB)

63.
Automated procedures for the Fluorescence Detector calibration at the Pierre Auger Observatory
Gaetano Salina, Andrej Filipčič, Gašper Kukec Mezek, Ahmed Saleh, Samo Stanič, Marta Trini, Darko Veberič, Serguei Vorobiov, Lili Yang, Danilo Zavrtanik, Marko Zavrtanik, 2015, objavljeni znanstveni prispevek na konferenci

Opis: The quality of the physics results, derived from the analysis of the data collected at the Pierre Auger Observatory depends heavily on the calibration and monitoring of the components of the detectors. It is crucial to maintain a database containing complete information on the absolute calibration of all photomultipliers and their time evolution. The low rate of the physics events implies that the analysis will have to be made over a long period of operation. This requirement imposes a very organized and reliable data storage and data management strategy, in order to guarantee correct data preservation and high data quality. The Fluorescence Detector (FD) consists of 27 telescopes with about 12,000 phototubes which have to be calibrated periodically. A special absolute calibration system is used. It is based on a calibrated light source with a diffusive screen, uniformly illuminating photomultipliers of the camera. This absolute calibration is performed every few years, as its use is not compatible with the operation of the detector. To monitor the stability and the time behavior, another light source system operates every night of data taking. This relative calibration procedure yields more than 2×10[sup]4 raw files each year, about 1 TByte/year. In this paper we describe a new web-interfaced database architecture to manage, store, produce and analyse FD calibration data. It contains the configuration and operating parameters of the detectors at each instant and other relevant functional parameters that are needed for the analysis or to monitor possible instabilities, used for the early discovery of malfunctioning components. Based on over 10 years of operation, we present results on the long term performance of FD and its dependence on environmental variables. We also report on a check of the absolute calibration values by analysing the signals left by stars traversing the FD field of view.
Ključne besede: Pierre Auger Observatory, Fluorescence Detector, detector calibration and monitoring, automated calibration procedure
Objavljeno v RUNG: 03.03.2016; Ogledov: 5443; Prenosov: 213
.pdf Celotno besedilo (1,06 MB)

64.
Studies in the atmospheric monitoring at the Pierre Auger Observatory using the upgraded Central Laser Facility
Carlos Medina-Hernandez, Andrej Filipčič, Gašper Kukec Mezek, Ahmed Saleh, Samo Stanič, Marta Trini, Darko Veberič, Serguei Vorobiov, Lili Yang, Danilo Zavrtanik, Marko Zavrtanik, 2015, objavljeni znanstveni prispevek na konferenci

Opis: The Fluorescence Detector (FD) at the Pierre Auger Observatory measures the intensity of the scattered light from laser tracks generated by the Central Laser Facility (CLF) and the eXtreme Laser Facility (XLF) to monitor and estimate the vertical aerosol optical depth (τ(z,t)). This measurement is needed to obtain unbiased and reliable FD measurements of the arrival direction and energy of the primary cosmic ray, and the depth of the maximum shower development. The CLF was upgraded substantially in 2013 with the addition of a solid state laser, new generation GPS, a robotic beam calibration system, better thermal and dust isolation, and improved software. The upgrade also included a back-scatter Raman LIDAR to measure τ(z,t). The new features and applications of the upgraded instrument are described. These include the laser energy calibration and the atmospheric monitoring measurements. The first τ(z,t) results and comparisons after the upgrade are presented using different methods. The first method compares the FD hourly response to the scattered light from the CLF (or XLF) against a reference hourly profile measured during a clear night where zero aerosol contents are assumed. The second method simulates FD responses with different atmospheric parameters and selects the parameters that provide the best fit to the actual FD response. A third method uses the new Raman LIDAR receiver in-situ to measure the back-scatter light from the CLF laser. The results show a good data agreement for the first and second methods using FD stations located at the same distance from the facilities. Preliminary results of τ(z,t) using the Raman LIDAR are presented as well.
Ključne besede: Pierre Auger Observatory, extensive air showers, the Fluorescence Detector, atmospheric monitoring, vertical aerosol optical depth, the Central Laser Facility, the eXtreme Laser Facility
Objavljeno v RUNG: 03.03.2016; Ogledov: 6218; Prenosov: 184
.pdf Celotno besedilo (3,96 MB)

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