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Thermal diffusivity downscaling of molybdenum oxide thin film through annealing temperature-induced nano-lamelle formation: a photothermal beam deflection study
S. Soumya, Vimal Raj, Mohanachandran Nair Sindhu Swapna, Sankaranarayana Iyer Sankararaman, 2021, izvirni znanstveni članek

Opis: The present work proposes a method of downscaling the thermal diffusivity (α) of MoO3 thin films through annealing temperature-induced nano-lamelle formation. The thermal diffusivity modification of the MoO3 films, prepared by the doctor blade method, is investigated by the sensitive transverse photothermal beam deflection technique. The X-ray diffraction analysis confirms the structural phase transformation from monoclinic to orthorhombic in the films annealed from 300 to 450 °C. The thermal induced anisotropy of the film is evident from the variation of the morphology index and texture coefficient. The field emission scanning electron microscopic analysis unveils the morphology modifications from blocks to the nano-lamelle structure with layers of average thickness ~ 77 nm. The thermal diffusivity measurement reveals a 53% reduction upon annealing the film to 450 °C. The drastic reduction is achieved through the annealing temperature-induced nano-lamelle formation and the phase transformation from monoclinic to orthorhombic in the MoO3 films.
Ključne besede: thermal diffusivity, molybdenum oxide, thin film, nano-lamelle, photothermal beam deflection
Objavljeno v RUNG: 04.07.2022; Ogledov: 1978; Prenosov: 27
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3.
Thermal diffusivity of molybdenum oxide nanowire film: a photothermal beam deflection study
Mohanachandran Nair Sindhu Swapna, 2021, izvirni znanstveni članek

Opis: The paper reports the preparation of thin film with MoO3 nanowires (NWs) by the doctor blade method and the study of its thermal diffusivity (α) by the sensitive photothermal beam deflection (PTD) method. When the Field Emission Scanning Electron Microscopic and Atomic Force Microscopic analysis unveil its morphology as NW bundles, the X-ray diffraction analysis reveals the structure to be orthorhombic. The NWs formed are of diameter ~ 20 nm and length up to 5 μm. The standardization of the transverse PTD setup is done by determining the value of α of iron, which agrees well with literature reports. The thermal diffusivity of MoO3 NW film is obtained as 0.0036 cm2 /s, which is 9.48% of its bulk counterpart. The reduction in the thermal diffusivity of NW makes it a suitable candidate for thermoelectric applications.
Ključne besede: Nanowires Molybdenum oxide Photothermal beam deflection Thermal diffusivity
Objavljeno v RUNG: 04.07.2022; Ogledov: 2002; Prenosov: 0
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4.
Evolution of fractal dimension in pulsed laser deposited MoO3 film with ablation time and annealing temperature
Mohanachandran Nair Sindhu Swapna, 2021, izvirni znanstveni članek

Opis: The multifractal analysis is a potential method for assessing thin flm surface morphology and its changes due to diferent deposition conditions and post-deposition treatments. In this work, the multifractal analysis is carried out to understand the surface morphology—root mean square (RMS) surface roughness—of nanostructured MoO3 flms prepared by pulsed laser deposition technique by varying the ablation time and post-deposition annealing. The XRD analysis shows the evolution of crystalline nature with annealing temperature. The XRD pattern of all the annealed flms shows the characteristic peak of the orthorhombic MoO3 phase. The FESEM and AFM analysis reveals the morphological modifcation with ablation time and annealing temperature. The multifractal analysis of the AFM images shows that the box—counting, information and correlation dimension varies with the annealing temperature. The study also reveals the inverse relation between the fractal dimension and the RMS surface roughness due to the annealing induced particle size variation and reorientation. The fractal dimension’s evolution in the pulsed laser deposited MoO3 flm with ablation time and annealing temperature is also investigated. Thus, the study reveals the potential of multifractal analysis in the thin flm surface characterizatio
Ključne besede: Multifractal analysis · Pulsed laser deposition · Molybdenum oxide · Atomic force microscopy · Fractal dimension
Objavljeno v RUNG: 04.07.2022; Ogledov: 2036; Prenosov: 0
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