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1.
Trajnostni biokompozitni materiali iz naravnih polimerov in njihova neporušna karakterizacija z optotermičnimi tehnikami
Mladen Franko, druga izvedena dela

Opis: Predstavljene so osnove zelene sinteze novih biokompozitnih materialov iz kombinacij celuloze s hitosanom ali keratinom in sporopoleninom ter njihove protimikrobne lastnosti in adsorpcijske sposobnosti za čiščenje vode. Pomembna lastnost biokompozitov z vidika njihove uporabnosti je tudi poroznost, ki jo lahko določamo neporušno in nekontaktno s tehniko optotermičnega odlkona. Ta omogoča določevanje toplotne difuzivnosti materialov ter preko nje poroznosti, kot tudi globinske porazdelitve v material vgrajenih snovi, ki izboljšujejo njegove lastnosti.
Ključne besede: Biokompoziti, celuloza, hitosan, keratin sporopolenin, toplotna difuzivnost, poroznost, optotermična spektrometrija
Objavljeno v RUNG: 11.05.2023; Ogledov: 1724; Prenosov: 0
Gradivo ima več datotek! Več...

2.
Optimized frequency dependent photothermal beam deflection spectroscopy
Mladen Franko, Dorota Korte, Humberto Cabrera, 2016, izvirni znanstveni članek

Opis: In the paper the optimization of the experimental setup for photothermal beam deflection spectrometry is performed by analyzing the influence of its geometrical parameters (detector and sample position, probe beam radius and its waist position etc) on the detected signal. Furthermore, the effects of fluid’s thermo-optical properties, for optimized geometrical configuration, on the measurement sensitivity and uncertainty determination of sample thermal properties is also studied. The examined sample is a recently developed CuFeInTe3 material. Results show, that it is a complex problem to choose the proper geometrical configuration as well as sensing fluid to enhance the sensitivity of the method. A signal enhancement is observed at low modulation frequencies by placing the sample in acetonitrile (ACN), while at high modulation frequencies the sensitivity is higher for measurements made in air. For both, detection in air and acetonitrile the determination of CuFeInTe3 thermal properties is performed. The determined values of thermal diffusivity and thermal conductivity are (0.048 ± 0.002) × 10−4 m2 s−1 and 4.6 ± 0.2 W m−1 K−1 and (0.056 ± 0.005) × 10−4 m2 s−1 and 4.8 ± 0.4 W m−1 K−1 for ACN and air, respectively. It is seen, that the determined values agree well within the range of their measurement uncertainties for both cases, although the measurement uncertainty is two times lower for the measurements in ACN providing more accurate results. The analysis is performed by the use of recently developed theoretical description based on the complex geometrical optics. It is also shown, how the presented work fits into the current status of photothermal beam deflection spectroscopy.
Ključne besede: Optitermi, na spektrometrija, toplotna difuzivnost, toplotna prevodnost, polprevodniki, vpliv topila
Objavljeno v RUNG: 07.11.2016; Ogledov: 5110; Prenosov: 0
Gradivo ima več datotek! Več...

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