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Naslov:NOVEL APPROACHES FOR THE DETERMINATION OF BIOGENIC AMINES IN FOOD SAMPLES
Avtorji:ID Franko, Mladen, UNG (Avtor)
ID Žorž, Mojca, UNG (Avtor)
ID Martelanc, Mitja, UNG (Avtor)
ID Budal, Sara, UNG (Avtor), et al.
Datoteke:.pdf 09rivoira_etal_103_122.pdf (441,06 KB)
MD5: BE164BF74F9489FB303B419144C6DB9F
 
Jezik:Angleški jezik
Vrsta gradiva:Delo ni kategorizirano
Tipologija:1.01 - Izvirni znanstveni članek
Organizacija:UNG - Univerza v Novi Gorici
Opis:In this work, new analytical approaches for determination of biogenic amines in wines were developed. For the first time, we studied the derivatization of BAs in wines with naphthalene- 2,3-dicarboxaldehyde (NDA) and with dabsyl chloride (DBS) and analysis of derivatized BAs by HPLC coupled to fluorescence (HPLC-NDA-FL) and thermal lens spectrometry (HPLC-DBS-TLS) detectors. The sensitivity of the two methods (LODs HPLC-NDA-FL in the range 27-73 μg/L; LODs HPLC-DBS-TLS in the range 3.4-11 μg/L) was higher than that of the official method for biogenic amines in wines, OIV-MA-AS315-18 (60-77 μg/L). For its best performances, the HPLC-DBS-TLS technique was applied to the analysis of putrescine, cadaverine, histamine and tyramine in two white wine samples. Additionally, exploiting the Berthelot reaction, the TLS fast screening of biogenic amines in wines, following the release of ammonia by transglutaminase, was also proposed. This approach allowed us to determine total biogenic amount content in concentrations below 0.1 mg/L, expressed as equivalents of histamine.
Ključne besede:biogenic amines, NDA, liquid chromatography, TLS, fluorescence, wine
Verzija publikacije:Objavljena publikacija
Leto izida:2017
Št. strani:103-122
Številčenje:62, 3
PID:20.500.12556/RUNG-3341-08936220-5988-0901-c97f-0e7cae85dcff Novo okno
COBISS.SI-ID:4945915 Novo okno
DOI:10.24193/subbchem.2017.3.08 Novo okno
NUK URN:URN:SI:UNG:REP:LNL6FETD
Datum objave v RUNG:02.11.2017
Število ogledov:5361
Število prenosov:278
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Gradivo je del revije

Naslov:Studia Universitatis Babes-Bolyai Seria Chemia
Skrajšan naslov:Studia UBB Chemia
Založnik:Babes Bolyai University
Leto izida:2017
ISSN:ISSN 2065-9520

Licence

Licenca:CC BY-NC-ND 4.0, Creative Commons Priznanje avtorstva-Nekomercialno-Brez predelav 4.0 Mednarodna
Povezava:http://creativecommons.org/licenses/by-nc-nd/4.0/deed.sl
Opis:Najbolj omejujoča licenca Creative Commons. Uporabniki lahko prenesejo in delijo delo v nekomercialne namene in ga ne smejo uporabiti za nobene druge namene.
Začetek licenciranja:01.11.2017

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