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Naslov:First utilization of magnetically-assisted photocatalytic iron ▫$oxide-TiO_2$▫ nanocomposites for the degradation of the problematic antibiotic ciprofloxacin in an aqueous environment
Avtorji:ID Radić, Josip (Avtor)
ID Žerjav, Gregor (Avtor)
ID Jurko, Lucija (Avtor)
ID Bošković, Perica (Avtor)
ID Fras Zemljič, Lidija (Avtor)
ID Vesel, Alenka (Avtor)
ID Mavrič, Andraž (Avtor)
ID Gudelj, Martina (Avtor)
ID Plohl, Olivija (Avtor)
Datoteke:URL https://www.mdpi.com/2312-7481/10/9/66
 
.pdf magnetochemistry-10-00066.pdf (14,48 MB)
MD5: 1B22D5BCBB658C61310F679F7BF4EA4B
 
URL https://www.mdpi.com/2312-7481/10/9/66/pdf
 
Jezik:Angleški jezik
Vrsta gradiva:Neznano
Tipologija:1.01 - Izvirni znanstveni članek
Organizacija:UNG - Univerza v Novi Gorici
Opis:The emergence of antimicrobial resistance due to antibiotics in the environment presents significant public health, economic, and societal risks. This study addresses the need for effective strategies to reduce antibiotic residues, focusing on ciprofloxacin degradation. Magnetic iron oxide nanoparticles (IO NPs), approximately 13 nm in size, were synthesized and functionalized with branched polyethyleneimine (bPEI) to obtain a positive charge. These IO-bPEI NPs were combined with negatively charged titanium dioxide NPs (TiO2@CA) to form magnetically photocatalytic IO-TiO2 nanocomposites. Characterization techniques, including X-ray diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM), infrared spectroscopy (IR), X-ray photoelectron spectroscopy (XPS), thermogravimetric analysis (TGA), electrokinetic measurements, and a vibrating sample magnetometer (VSM), confirmed the successful formation and properties of the nanocomposites. The nanocomposites exhibited a high specific surface area, reduced mobility of photogenerated charge carriers, and enhanced photocatalytic properties. Testing the photocatalytic potential of IO-TiO2 with ciprofloxacin in water under UV-B light achieved up to 70% degradation in 150 min, with a degradation rate of 0.0063 min−1. The nanocomposite was magnetically removed after photocatalysis and successfully regenerated for reuse. These findings highlight the potential of IO-TiO2 nanocomposites for reducing ciprofloxacin levels in wastewater, helping curb antibiotic resistance.
Ključne besede:photocatalytic degradation, magnetic iron oxide-TiO2 nanocomposites, hetero-agglomeration, multifunctionality, antibiotic ciprofloxacin, antimicrobial resistance
Status publikacije:Objavljeno
Verzija publikacije:Objavljena publikacija
Datum objave:01.01.2024
Leto izida:2024
Št. strani:str. 1-29
Številčenje:Vol. 10, issue 9, [article no.] 66
PID:20.500.12556/RUNG-9294-b9756487-c9bd-398f-71c2-a2d47910690c Novo okno
COBISS.SI-ID:206740739 Novo okno
UDK:54
ISSN pri članku:2312-7481
eISSN:2312-7481
DOI:10.3390/magnetochemistry10090066 Novo okno
NUK URN:URN:SI:UNG:REP:MGCS7LBX
Datum objave v RUNG:09.09.2024
Število ogledov:565
Število prenosov:6
Metapodatki:XML DC-XML DC-RDF
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Gradivo je del revije

Naslov:Magnetochemistry
Skrajšan naslov:Magnetochemistry
Založnik:MDPI AG
ISSN:2312-7481
COBISS.SI-ID:526327577 Novo okno

Gradivo je financirano iz projekta

Financer:ARIS - Javna agencija za znanstvenoraziskovalno in inovacijsko dejavnost Republike Slovenije
Program financ.:Raziskovalni program
Številka projekta:P2-0412

Licence

Licenca:CC BY 4.0, Creative Commons Priznanje avtorstva 4.0 Mednarodna
Povezava:http://creativecommons.org/licenses/by/4.0/deed.sl
Opis:To je standardna licenca Creative Commons, ki daje uporabnikom največ možnosti za nadaljnjo uporabo dela, pri čemer morajo navesti avtorja.
Začetek licenciranja:06.09.2024

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