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3. Speckle interferometric investigation of argon pressure-induced surface roughness modifications in RF-sputtered MoO[sub]3 filmS. Soumya, R. Arun Kumar, S. Sreejyothi, Vimal Raj, Mohanachandran Nair Sindhu Swapna, Sankaranarayana Iyer Sankararaman, 2021, original scientific article Abstract: Film quality analysis is of more considerable signifcance due to its diversifed applications in various felds of technology.
The present work reports the speckle interferometric analysis of the argon pressure-induced surface roughness modifcations
of RF sputtered MoO3 flms. The paper suggests a new method of surface quality analysis of thin flms through a parameter
δ, which is the diference between the initial and fnal inertia moment values in the study of the thermal-induced dynamic
speckle pattern. The limitations of root mean square surface roughness analysis of the atomic force microscopic image of the
flms is also exemplifed. The research suggests that argon pressure plays a vital role in the surface property of RF sputtered
flms and also that the dynamic speckle analysis can give precise information about the quality of flms. The contour plot of
particle displacement vector under thermal stress, suggests the degree of uniformity in the distribution of particles in the flm.
Keywords: speckle pattern interferometry, time history of speckle pattern, cross correlation, inertia moment
Published in RUNG: 04.07.2022; Views: 1180; Downloads: 0
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4. Thermal diffusivity downscaling of molybdenum oxide thin film through annealing temperature-induced nano-lamelle formation: a photothermal beam deflection studyS. Soumya, Vimal Raj, Mohanachandran Nair Sindhu Swapna, Sankaranarayana Iyer Sankararaman, 2021, original scientific article Abstract: The present work proposes a method of downscaling the thermal diffusivity (α)
of MoO3 thin films through annealing temperature-induced nano-lamelle formation. The
thermal diffusivity modification of the MoO3 films, prepared by the doctor blade method,
is investigated by the sensitive transverse photothermal beam deflection technique. The X-ray diffraction analysis confirms the structural phase transformation from monoclinic to
orthorhombic in the films annealed from 300 to 450 °C. The thermal induced anisotropy of
the film is evident from the variation of the morphology index and texture coefficient. The
field emission scanning electron microscopic analysis unveils the morphology modifications
from blocks to the nano-lamelle structure with layers of average thickness ~ 77 nm. The
thermal diffusivity measurement reveals a 53% reduction upon annealing the film to 450 °C.
The drastic reduction is achieved through the annealing temperature-induced nano-lamelle
formation and the phase transformation from monoclinic to orthorhombic in the MoO3 films.
Keywords: thermal diffusivity, molybdenum oxide, thin film, nano-lamelle, photothermal beam deflection
Published in RUNG: 04.07.2022; Views: 1130; Downloads: 26
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