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Photothermal techniques in environmental analysis
Korte Dorota, other performed works

Keywords: photothermal measurements, thermal lens spectrometry
Published in RUNG: 21.04.2023; Views: 126; Downloads: 0
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Effect of duty cycle on photothermal phenomenon – a thermal lens study
Swapna Mohanachandran Nair Sindhu, 2019, original scientific article

Keywords: Photothermal phenomena Thermal lens technique Optical chopper Duty cycle variation
Published in RUNG: 05.07.2022; Views: 477; Downloads: 0
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Time series analysis of duty cycle induced randomness in thermal lens system
Swapna Mohanachandran Nair Sindhu, 2020, original scientific article

Abstract: The present work employs time series analysis, a proven powerful mathematical tool, for investigating the complex molecular dynamics of the thermal lens (TL) system induced by the duty cycle (C) variation. For intensity modulation, TL spectroscopy commonly uses optical choppers. The TL formation involves complex molecular dynamics that vary with the input photothermal energy, which is implemented by varying the duty cycle of the chopper. The molecular dynamics is studied from the fractal dimension (D), phase portrait, sample entropy (S), and Hurst exponent (H) for different duty cycles. The increasing value of C is found to increase D and S, indicating that the system is becoming complex and less deterministic, as evidenced by the phase portrait analysis. The value of H less than 0.5 conforms the evolution of the TL system to more anti-persistent nature with C. The increasing value of C increases the enthalpy of the system that appears as an increase in full width at half maximum of the refractive index profile. Thus the study establishes that the sample entropy and thermodynamic entropy are directly related.
Keywords: Time series analysis Fractal analysis Photothermal lens spectroscopy Fractal dimension Hurst exponent Sample entropy
Published in RUNG: 05.07.2022; Views: 456; Downloads: 0
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Thermal diffusivity downscaling of molybdenum oxide thin film through annealing temperature-induced nano-lamelle formation: a photothermal beam deflection study
S. Soumya, Vimal Raj, Mohanachandran Nair Sindhu Swapna, Sankaranarayana Iyer Sankararaman, 2021, original scientific article

Abstract: The present work proposes a method of downscaling the thermal diffusivity (α) of MoO3 thin films through annealing temperature-induced nano-lamelle formation. The thermal diffusivity modification of the MoO3 films, prepared by the doctor blade method, is investigated by the sensitive transverse photothermal beam deflection technique. The X-ray diffraction analysis confirms the structural phase transformation from monoclinic to orthorhombic in the films annealed from 300 to 450 °C. The thermal induced anisotropy of the film is evident from the variation of the morphology index and texture coefficient. The field emission scanning electron microscopic analysis unveils the morphology modifications from blocks to the nano-lamelle structure with layers of average thickness ~ 77 nm. The thermal diffusivity measurement reveals a 53% reduction upon annealing the film to 450 °C. The drastic reduction is achieved through the annealing temperature-induced nano-lamelle formation and the phase transformation from monoclinic to orthorhombic in the MoO3 films.
Keywords: thermal diffusivity, molybdenum oxide, thin film, nano-lamelle, photothermal beam deflection
Published in RUNG: 04.07.2022; Views: 432; Downloads: 22
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